Vacuum drying oven principle and common problems - Database & Sql Blog Articles

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Vacuum drying oven working principle and analysis of common problems

1. The reason why the meter reading of the vacuum drying box differs from the reading of the glass rod thermometer in the vacuum chamber: The general electric heating vacuum drying box adopts the method of heating the wall surface of the vacuum chamber first and then irradiating the workpiece by the wall. In this way, the temperature sensor of the temperature control meter can be arranged on the outside wall of the vacuum. The sensor can accept convection, conduction, and radiant heat simultaneously. The glass rod thermometer in the vacuum chamber can only receive radiant heat, and because the blackness of the glass rod cannot reach 1, a considerable part of the radiant heat is refracted, so the temperature value reflected by the glass rod thermometer is definitely lower than the temperature reading of the meter. . In general, it is normal to have a difference between the temperature reading of the meter and the reading of the glass rod thermometer within 30 °C at 200 °C. If the temperature sensor of the temperature control instrument is placed in the vacuum chamber, the difference between the temperature value of the glass rod thermometer and the temperature reading of the meter can be appropriately reduced, but it is impossible to eliminate, and the sealing reliability of the vacuum chamber increases a possible unreliable link. . If you do not want to see this difference from the practical point of view, you can use the display correction function unique to the temperature control instrument.

2. The reason why the vacuum drying box first vacuums and then heats up

1) If the heating air is pumped out by the vacuum heating and then the vacuum is pumped out, the heat will be brought to the vacuum pump, which will cause the vacuum pump to rise too high, which may reduce the efficiency of the vacuum pump.

2) The heated gas is directed to a vacuum gauge, and the vacuum gauge produces a temperature rise. If the temperature rise exceeds the operating temperature range specified by the vacuum gauge, the vacuum gauge may cause an indication error. The correct method of use should first vacuum and then heat up. After the rated temperature has been reached, if it is found that the degree of vacuum has decreased, then add it appropriately. This is advantageous for extending the life of the device.

3) The workpiece is placed in a vacuum box to evacuate the vacuum to remove the gas components that can be removed from the workpiece material. If the workpiece is heated first, the gas expands when heated. Due to the excellent sealing of the vacuum box, the enormous pressure generated by the expanding gas may cause the observation window tempered glass to burst. This is a potential danger. This danger can be avoided by following the procedure of first vacuuming and then heating up the heating.

3. The reason why the temperature uniformity parameter is not set in the vacuum drying oven

The general electric (blast) drying ovens are equipped with temperature uniformity parameters: the natural convection drying oven is the upper limit of the operating temperature multiplied by 3%, and the forced convection drying oven is the upper limit of the operating temperature multiplied by 2.5%. However, the electric vacuum drying oven does not have a temperature uniformity parameter. Why? There is almost no possibility of relying on the movement of gas molecules in the vacuum oven to make the temperature of the studio uniform. Therefore, conceptually we can no longer use the temperature uniformity defined by the usual electric (blast) drying oven to the vacuum drying oven. It is also meaningless to set this indicator under vacuum. The amount of thermal radiation is inversely proportional to the square of the distance. For the same object, the radiant heat received at 20 cm from the heated wall is only 1/4 of 10 cm from the heated wall. big difference. This phenomenon is warm when the sun is shining in the winter, and the sun is not warm. It is a truth that the sun is not cold. Because the vacuum drying oven is difficult to make the radiant heat of each point in the three-dimensional space of the studio uniform and lacks an authoritative evaluation method, it may be that the temperature uniformity parameter is not included in the standard of the electric vacuum drying oven. s reason.

First, the structural characteristics:

1. The inner body of the box is made of mirror stainless steel plate or wire drawing argon arc welding. The outer shell is made of high quality cold-rolled steel plate and electrostatically sprayed. The shape is beautiful and novel.

2. The insulation system is filled with ultra-fine glass fiber insulation zone, and the inner and outer joints are made of non-metal high temperature resistant materials, which effectively reduce the temperature conduction.

3. The circuit system side is opened by a door to facilitate maintenance and overhaul.

4. The door can be closed tightly and can be adjusted. The integrally formed silicone rubber sealing ring ensures high vacuum inside the box.

5. Storage, heating, testing and drying are carried out in an environment free of oxygen, so they are not oxidized.

6. The rectangular body studio maximizes the effective volume.

7. The tempered and bulletproof double-glazed doors are used to observe the objects in the working room at a glance.

8. Microcomputer temperature controller with timing function, accurate and reliable temperature control.

Second, the control system:

1. Adopt touch button temperature controller, digital display LED display, PID intelligent control instrument;

2. Pt100 platinum resistance temperature sensor;

3. Control mode: heat balance temperature adjustment mode; Third, protection system: protection system consists of over temperature protection and alarm device. The integrity of the components and test pieces is guaranteed.

Shangyu Star Equipment Co., Ltd.

Located in Daoxu Town, Shangyu District, Shaoxing City, Zhejiang Province, it is an enterprise integrating production, product research and development, processing and trade. The company's main products: drying box series, incubator series, laboratory muffle furnace series, distilled water series, as well as clean workbench, air shower, fume hood, biological safety cabinet and other complete purification equipment.

The company has a strong technical research and development team, a strong after-sales guarantee service system, is the leader in China's laboratory complete sets of equipment manufacturers, welcome customers to buy.